Rhodium
(Chief Bee)
09-10-03 01:01
No 457993
      Microscale Column Chromatography
(Rated as: good read)
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Manual Microscale Column Chromatography Pressurization Apparatus
Bruce W. Baldwin
J. Chem. Educ. 80, 1182 (2003) (../rhodium/pdf /microscale.column.chromatography.pdf)

Abstract

Pressurization of a Pasteur pipet for microscale chromatography is simplified by connecting a 20- or 30-mL syringe to the pipet using a length of Tygon tubing. This simple system allows the student to easily dry-pack a column using common chromatography packing materials. Results were uniformly good for introductory, organic, or upper-division research chemistry students.