Vibrating_Lights
(Hive Bee) 10-25-01 01:17 No 228479 |
where does the halogen go in the Bomb | Bookmark | ||||||
Where does the halogen go in the bomb with halosafrole and MeAm |
||||||||
goiterjoe (Hive Addict) 10-25-01 01:26 No 228484 |
Re: where does the halogen go in the Bomb | Bookmark | ||||||
It should pick up a hydrogen from the methylamine to produce the hydrochloric acid. Sed quis custodiet ipsos custodes? |
||||||||
Vibrating_Lights (Hive Bee) 10-25-01 02:30 No 228498 |
Re: where does the halogen go in the Bomb | Bookmark | ||||||
If idio is used then it will produce HI Correct. How could you go about extracting it. Will the post reaction A/B with NaOH convert the HI to NaI which could be extracted from the remaining polar mix with acetone after evaporation and saved for a later time. This reaction seems pretty efficent. |
||||||||
Bwiti (Hive Addict) 10-25-01 07:42 No 228589 |
Re: where does the halogen go in the Bomb | Bookmark | ||||||
"This reaction seems pretty efficent." I don't think it is. You'll get much better yields if you use an azide as the nucleophile, instead of ammonia or methylamine. All you need to do is reduce the safrole-azide with Mg or calcium. Total Synthesis 2 has all the info on this reaction that you need. The christian god hates your soul. Care for a little necrophilia? |
||||||||