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PolytheneSam
(Master Searcher)
12-07-01 02:12
No 245138
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LiBr Russian patent abstract
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Can someone translate this?<br><br><img src="../picproxie_docs/000245138-file_6ya2.jpg"><br><hr>http://www.geocities.com/dritte123/PSPF.<wbr>html
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dovlatov<br>
<i>(<span title="The user's title at the time of posting">Hive Bee</span>)</i><br>
<span title="Posting date">12-07-01 05:07</span><br>
<span title="Link to this post by using the markup [245181]">No 245181</span><br>
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<title>Re: LiBr Russian patent abstract
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(references)<br>Y.I. Matyushenko, V.A. Morozova & S.M. Tulskii<br>1. A METHOD FOR PRODUCING LITHIUM BROMIDE, beginning by refining a lithium carbonate suspension with an aqueous bromide in the presence of an inorganic reagent, the subsequent separation of mixture from sediment, it's evaporation and crystallization from the product, differentiated so, that, the cost of the process is deliberately lowered by enhancing yields and conserving the basic qualitative product. As an inorganic reagent ammoniated water is used. <br>2. Re: Method no. 1, it is significant that ammoniated water is used at a concentration of 25-30%<br>3. Re: Method no. 1, it is significant that the refinement with aqueous bromide is initiated at a rate of 60-90 liters/hour maintaining lithium carbonate ratio in the reactive mass at 60-90 grams/liter. After that a rate of 30-50 liters/hour in the presence of said lithium carbonate.<br><br>..apologies to more technically literate Russian bees...<br>dovlatov.<br>
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Bwiti<br>
<i>(<span title="The user's title at the time of posting">PVC-Analog Taste-Tester</span>)</i><br>
<span title="Posting date">12-07-01 05:29</span><br>
<span title="Link to this post by using the markup [245187]">No 245187</span><br>
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<b title="The subject of this post">Re: LiBr Russian patent abstract</b>
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Damn, I didn't know that producing lithium bromide would be that much of a pain in the ass. Boiling it with benzoic acid produces HBr, so it's worth it!<img src="../forum/images/icons_lightgrey/cool.gif" alt="cool" title="Cool" heigth="15" width="15"><br><hr> Split a piece of wood and I am there. Lift a stone and you will find me.
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uemura<br>
<i>(<span title="The user's title at the time of posting">Hive Bee</span>)</i><br>
<span title="Posting date">12-07-01 12:27</span><br>
<span title="Link to this post by using the markup [245265]">No 245265</span><br>
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<b title="The subject of this post">Re: LiBr Russian patent abstract</b>
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Bwiti,<br><blockquote title="Quoted text"><hr><p>Damn, I didn't know that producing lithium bromide would be that much of a pain in the ass<p><hr></blockquote><p><br>You could simple try this one:<br>Li2CO3 + 2HBr -> 2 LiBr + H2O + CO2<br>evap water until cristalls appear, suction filter, dry in evac desic, put in thightly sealed bottle because it's a bit hygroscopic. <hr> Carpe Diem
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Bwiti<br>
<i>(<span title="The user's title at the time of posting">PVC-Analog Taste-Tester</span>)</i><br>
<span title="Posting date">12-07-01 16:20</span><br>
<span title="Link to this post by using the markup [245306]">No 245306</span><br>
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<b title="The subject of this post">Re: LiBr Russian patent abstract</b>
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"it's a bit hygroscopic."<br><br> If I can keep methylamine hydrochloride dry, then lithium bromide won't be a problem. <br> Hmmmm, how much does benzoic acid cost these days? 10oz for like $12? Pet ether's cheap..Fuck making bromosafrole with DMSO; Smells like human waste and rotten milk. Peace! <br><img src="../forum/images/icons_lightgrey/cool.gif" alt="cool" title="Cool" heigth="15" width="15"><br><hr> Split a piece of wood and I am there. Lift a stone and you will find me.
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