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ChemicalSolution (Newbee) 12-24-01 23:30 No 250342 |
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Can some bee point me to a procedure for converting Et-Br to ethylamine using the Delipine reaction? I realize this procedure works much better with NaI but Et-Br is all this bee has to work with. Thanks--CH ![]() |
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ChemicalSolution (Newbee) 12-24-01 23:33 No 250343 |
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Should also add.. SWIM wishes to convert Et-amine to tri ethyl amine. Can this be done by refluxing Et-amine in IP-OH with an abundance of Et-Br like what would be done in the Bromosafrole reaction with NH3 only the higher amine is prefered. Thanks!! CH ![]() |
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element109 (Hive Bee) 12-25-01 06:14 No 250388 |
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The Delepine probably only work well with iodides . So you'll have to reflux with NaI in acetone first. And your idea will probably give you chiefly the quaternary salt. Why don't you just buy triethylamine? e109 |
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Rhodium (Chief Bee) 12-25-01 13:24 No 250429 |
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Re: Delepine with Et-Br | Bookmark | |||||
The Delepine works well with the bromides if NaI is added to the refluxing reaction mixture. |
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