Bwiti
(PVC-Analog Taste-Tester) 08-12-02 01:11 No 344577 |
Storage of Ethyl Bromide? | Bookmark | ||||||
Besides the usual "should be stored in a cool, dry, well-ventilated area in tightly sealed containers", is there anything else I should know about storage of this chem? Is there something I could add to home-made ethyl bromide to preserve it for a few months? Love my country, fear my government. |
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hypo (Official Hive Approximator) 08-12-02 01:19 No 344578 |
very tightly! | Bookmark | ||||||
it should be stored in very tightly sealed containers! i had evaporate 20 ml into the lab atmosphere over some months . if you used drones method, you should shake it with 1/5th volume of conc. H2SO4 to remove possible ether and then wash with sodium (bi)carbonate and water. it should be realtively stable, distill before use. couch terrorist |
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Bwiti (PVC-Analog Taste-Tester) 08-12-02 01:44 No 344582 |
This compound will be fun to work with . | Bookmark | ||||||
This compound will be fun to work with[sarcasm]. Thanks for the heads-up! Love my country, fear my government. |
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Osmium (Stoni's sexual toy) 08-12-02 02:05 No 344585 |
Alkyl halogenides are often stored over a piece ... | Bookmark | ||||||
Alkyl halogenides are often stored over a piece of silver foil. Dunno why though. I'm not fat just horizontally disproportionate. |
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Ritter (Master Whacker) 08-12-02 05:12 No 344604 |
Silver in alkyl halides | Bookmark | ||||||
I'm not exactly sure of the mechanism, however storing alkyl halides with a small amount of silver wire or copper shot prevents discoloration and decomposition of the organics. For example, I have seen numerous bottles of alkyl iodides from Aldrich, the most recent reagents were all shipped with a few copper beads(shot) rolling around in the bottom of the bottle. The copper has completely prevented any discoloration from forming over a 5 year period. |
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hest (Hive Addict) 08-12-02 23:58 No 344997 |
Ethylbromide | Bookmark | ||||||
I have a 25L flask from the 1950's still nice and clear. It's just standing in a basment. |
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