![]() |
![]() |
|||||||
twodogs
(Stranger) 10-17-02 03:16 No 369562 |
![]() |
Hydroxylamine Hydrochloride | Bookmark | |||||
200 gms nitromethane, 300 gms 28% HCl and 300 gms Glacial Acetic Acid were mixed and slowly heated to just below reflux and temp held there for about 4 hours then temp adjusted for relux and left for 12 hours. Left to cool for 8 hours. Crystals formed. Liquid was decanted and reduced to about 200 mls and put in freezer overnight. More crystals were recovered. Total yield 100 gms. Crystals became yellowish on standing. |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
Tricky (Stunning) 10-17-02 03:43 No 369566 |
![]() |
O! | Bookmark | |||||
I think it's gibberish. It's impossible. Wanna make laugh the GOD? - Tell him about your plans. |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
karl (Hive Bee) 10-17-02 04:01 No 369572 |
![]() |
Nitromethane has a nitrogen in the fifth ... | Bookmark | |||||
Nitromethane has a nitrogen in the fifth oxidation state while hydroxylamine in the third. How is the nitromethane being reduced by GAA. I doubt the acetic acid could be so readily oxidised. |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
moo (Hive Bee) 10-17-02 04:49 No 369578 |
![]() |
Let's not be hasty | Bookmark | |||||
Please read Post 263772 (halfapint: "Re: Nitrostyrene or Nitropropene electrochem reduction", Chemistry Discourse) and Post 285259 (uemura: "Oldie, but Goodie", Novel Discourse). |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
twodogs (Stranger) 10-18-02 04:11 No 369911 |
![]() |
O! | Bookmark | |||||
Say what?? |
||||||||
![]() |
![]() |
|||||||