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synthesys
(Stranger) 05-01-03 17:56 No 430613 |
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safrole gone bad? | Bookmark | |||||
Swim is right on the money with wacker O2 all the time, consistent 85% yields, bisulfate test real solid, the works... Until last week ![]() But on the bisulfate... Well, there was some solid, but the majority of the oil just sat there...WTF ... I was so surprised, that I reran the bisulfate test again, but got the same result. There are two possible variables: 1. safrole that has been sitting around at RT for a few months has gone bad. ![]() ![]() ![]() 2. The ketone is still a ketal, and was not hydrolized properly. ![]() Anybody? |
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GOD (Hive Addict) 05-01-03 23:00 No 430674 |
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swim has seen safrole that sat at room temp... | Bookmark | |||||
swim has seen safrole that sat at room temp (in clear glass containers) turn from a crystal-clear to an off-yellow color in a matter of a few weeks. Wouldnt suprise swim if that wasnt the problem (although he knows nothing of the O2 wacker). shit...I found out it was all just one big manic episode! |
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FriendlyFinger (Hive Bee) 05-02-03 04:28 No 430718 |
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Swim has some safrole in a clear glass ... | Bookmark | |||||
Swim has some safrole in a clear glass container kept in a white foam box, so it is exposed to some light which has just started to get a hint of yellow, after 2 years. Regards, FF |
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abolt (Hive Bee) 05-02-03 06:11 No 430724 |
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Post 390702 | Bookmark | |||||
Post 390702 (abolt: "Old Sassafras", General Discourse) when we forget to pray for the angels, the angels forget to pray for us! |
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DjTime (Newbee) 07-29-03 23:15 No 450600 |
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Swim has a sassy ??? | Bookmark | |||||
I have a bottle of sassy around 1L . It has a really golden yellow color to it. It's been sitting at around 60-90 F for about 8 months. It also has water in it, looks alot like when you put oil and vineager together. Will that be ok if I distill it like normal??? |
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baalchemist (Chef d'Equippe) 07-30-03 04:03 No 450646 |
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It'll be just fine after a distillation. | Bookmark | |||||
It'll be just fine after a distillation. GODISNOWHERE Shoot Narcs, Not Drugs |
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