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navarone
(Stranger)
08-27-04 06:02
No 527686
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HI from DECALIN !!!!
(Rated as: good read)
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ApprenticeCook
(Hive Addict)
08-27-04 07:58
No 527730
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huh?
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Ok when you find a decent source for DECALIN with a relativly low price, providing a decent amount which is rather purified for use in such a method tell us..
Sounds like this will cost heaps and not be as effective (both cost wise and yield wise) as proven, established methods.
Otherwise for HI generation ill stick to the good old methods that work fine with very little work involved. Not to mention they cost shit all aswell....
-AC
Its just my opinion, but no-one listens to me anyway, and rightly so...
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Nicodem
(Hive Bee)
08-27-04 16:14
No 527780
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Organikum once suggested tetraline for HI...
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Organikum once suggested tetraline for HI (re)generation from iodine. See Post 499395 (Organikum: "Times ago Piglet suggested the use of Zn/I for", Stimulants) and the replies. Which also means that decaline oxidation with iodine does not stop at the tetraline stage.
Navarone, do you mind adding a reference/link to that decaline oxidation you suggested. How is anybee supposed to consider your idea without seeing what it is about? Besides, decaline is not an aromatic compound as you say. Tetraline, the product, as well naphtalene are aromatics. Also nitrogen or argon are not catalysts, they just provide an inert atmosphere so the HI does not oxidise (get redish). Also, why would you want to prepare aqueous HI when (I suspect) you want to use it for pseudoephedrine reduction. It would be more wise to simply oxidise decaline or tetraline in acetic acid which would give you an HI solution in acetic acid perfect for further use (decaline, tetraline and naphtalene are inert in the ephedrine reduction reaction).
“The real drug-problem is that we need more and better drugs.” – J. Ott
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Organikum
(Wonderful Personality)
08-28-04 00:26
No 527843
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Iodine + tetraline is a well-referenced methop
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Iodine + tetraline is a well-referenced methop from inorganic chemistry. Iodine + copaia oil works too. Iodine + rosin works too, mix with at least equal amount of sand.
All three methods can end in an impressive explosion, including a cinemascope fireball and more if done wrong. Say to much heat, to fast heating to much iodine added at once.... ....multiple ways to fuck this up.
Be warned. ORG
so near, so far......
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