03-31-01 09:29
No 181193
SWIM followed MM writeup and threw in some nitroethane instead of nitromethane, 25ml's instead of 20. The reaction went really smooth didnt choke the condensor at an addition rate of 3-4 drops per second. 25g of ketone was used, 30g Al, allowed to spin for 2h after addition was finished. basified, extracted, washed, dried and gassed to get a little over 20g of the hydrochloride. SWIM is sure you all already knew this but what the heck, boredom struck and SWIM felt like typing it out anyways :(
I like to cook!
(Hive Bee)
04-02-01 08:15
No 181621
did you make or buy the nitroethane?
(Hive Bee)
04-02-01 10:41
No 181648
the neighbors cat sorta bought it for company reasons, in excess, NitroE was tested and Xtra basically given to the cat. cats are evil i tell you! evil!
I like to cook!