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Vibrating_Lights
(Hive Bee) 02-10-02 01:46 No 267557 |
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vaccume induced crystalization | Bookmark | |||||
If one were to have some freshly distilled, weighed freebase in a recieving flask, could one not simply add the equimolar ammount of 38%Hcl then stir under vaccume to induce crystylazation with further desication of the product. Vl_ |
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LaBTop (Daddy) 02-10-02 02:31 No 267569 |
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Re: vaccume induced crystalization | Bookmark | |||||
Some parts of your freebase will certainly not like you and leave. You will need a solvent to dilute your acids in, to safely form your salts. LT/ WISDOMwillWIN |
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Chromic (Hive Addict) 02-10-02 02:41 No 267573 |
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Re: vaccume induced crystalization | Bookmark | |||||
Have the freebase in a non-polar, extract with acidic water (until pH 4), then boil off the water. Don't add concentrated HCl to your freebase. |
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Vibrating_Lights (Hive Bee) 02-10-02 02:48 No 267578 |
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Re: vaccume induced crystalization | Bookmark | |||||
Those md s that make the red colors Lt_ Ether is the choice. Terbium you were right. Ice bath on the gassing flask ensures 0 solubility of the HCL salt. VL_ |
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