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PurpleSmurf
(Stranger) 03-02-02 12:48 No 275875 |
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Enthanol in Wacker | Bookmark | |||||
Can Ethanol be substituted for methanol or DMF in the Wacker oxidation, with no other alterations in chemicals or procedure? Thanks a bunch |
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Ritter (Master Whacker) 03-02-02 14:30 No 275921 |
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Re: Enthanol in Wacker | Bookmark | |||||
Ethanol has been used successfully in O2 Wacker oxidations. |
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Sunlight (Pioneer Researcher) 03-02-02 17:10 No 275973 |
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Re: Enthanol in Wacker | Bookmark | |||||
But with pressure right ? |
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PurpleSmurf (Stranger) 03-02-02 17:41 No 275994 |
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Re: Enthanol in Wacker | Bookmark | |||||
Why would pressure be required? Ethanol boils at a higher temperature than methanol, is there something I'm missing here? |
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Vibrating_Lights (Hive Bee) 03-03-02 06:48 No 276234 |
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Re: Enthanol in Wacker | Bookmark | |||||
There are two different O2 wackers. One uses pressurized O2. VL_ |
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Ritter (Master Whacker) 03-04-02 11:42 No 276783 |
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Re: Enthanol in Wacker | Bookmark | |||||
Sunlight: Yes medium pressure was used- 50 to 100 psi. Reactor was initially charged to 100psi and recharged after it dropped to 50psi. |
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