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Archaeoptrix
(Hive Bee) 05-07-02 23:11 No 305904 |
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7%soln->HgI2? | Bookmark | |||||
Hey Everybody, Got 1 gal. solution of ... 7% iodine 80% ipa 13% h2o From the notes I've read here...to make enough HgI2 for a 1x MM alhg, one plops .3-.5g Hg (l) into a 30ml solution of 2% iodine tincture...shake and bake. Now, my questions are... 1) I'm sure I should use 99% ipa to dillute the solution down to 2%, no? Any other suggestions...MeOH or EtOH? 2) After the solution is dilluted down to 2% iodine, its still going to be ~3-4% water. Is this going to be a problem adding this extra h2o to a 1x MM al-hg rxn.? Cheers...a Load"*",8,1 |
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halfapint (Ubiquitous Precursor Medal Winner) 05-08-02 03:27 No 306008 |
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Why dilute? | Bookmark | |||||
My version of this product contains no added water, just 99% isopropanol. I see no reason to perform any dilution: your solution is of greater purity than the 2% tincture, so why adulterate it? The formulaic procedure you are following, is adapted to the availability of the less desirable merchandise. Plop your Hg in, see it happen. a half a pints a half a pound a half a world a half a round Sidearm n. Flask neck tube. |
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Archaeoptrix (Hive Bee) 05-14-02 23:25 No 308516 |
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to get h2o% down a bit | Bookmark | |||||
Thanks for the advice halfapint...I was intending to dillute the 7% down to make it fit rxn. guidelines but I was also concerned about getting the h2o % down a bit as well...any comments? thanks...a Load"*",8,1 |
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