06-26-02 20:22
No 325709
While reading P2P synthesis from chloroacetone on Rhodium's site I came up with an idea for this synthesis.
1,3-benzodioxole + chloroacetone --> MDP2P
If it works with benzene I think it should work with 1,3-benzodioxole too. The only problem are the yields, which are kinda low with benzene. Any comments or suggestions?
Life without chemistry would be a mistake.
(Stranger)
06-26-02 20:28
No 325710
Or yould could also use the Mn(III) catalyzed version, but in both cases you'll also end up with the 2,3-methylenedioxy-P2P.
(Hive Bee)
06-26-02 20:38
No 325714
How can 2,3-MDP2P be separated from 3,4-MDP2P? Would a fractional vacuum distillation work? What is the boiling point of 2,3-MDP2P?
Life without chemistry would be a mistake.
(Hive Bee)
06-26-02 21:55
No 325734
If you read TSII, then you'd know that AlCL3 tears the methylenedioxy ring all to shit. The 1,3 benzodioxole+chloroacetone synth can never work.
Do not go gentle into that good night. Rage, Rage, against the dying of the light. --Dylan Thomas