11-30-02 22:16
No 384994
2c-h hcl dissolved in glacial acetic acid + br2 -> 2c-b hbr
Would this workout fine? Or would freebasing 2c-h hcl give some serious advantages over this method?
(Chief Bee)
12-01-02 01:14
No 385035
It works all right as long as you take the time to do what's necessary to clean up the hydrobromide salt without going through the freebase stage. The bromination creates a whole lot of very dark by-products.
Suggested procedure: ../rhodium /2cb.bro