tropine (Stranger)
10-17-03 13:53
No 465264
      will meth freebase come off with toluene in     

a vaccuum assisted rotovap?  Toluene does have quite high bp. so I am worried that in the rotovap, the meth freebase will distill off with the toluene?
 
 
 
 
    starlight
(Hive Bee)
10-17-03 14:52
No 465282
      bps are very different     

so long as you are not pulling too low a vacuum you should be ok.

what type of pump are you using and what vacuum does it achieve?
 
 
 
 
    Midi
(Newbee)
10-17-03 23:52
No 465356
      Tolulene boiling point     

Toulene bp - 110.6

What is freebase meths bp?

http://www.greenspun.com/bboard/q-and-a-fetch-msg.tcl?msg_id=00749A
 
 
 
 
    Rhodium
(Chief Bee)
10-18-03 07:31
No 465412
      Methamphetamine boiling point     

The boiling point of methamphetamine at atmospherical pressure is 209-210°C, so it is very easy to separate from toluene, as long as you do not use excessive vacuum and heat.