jaws (Newbee)
11-21-02 20:44
No 382117
      can palladium chloride be made...  Bookmark   

Can palladium chloride be made from a piece of palladium metal?

Jaws tried to UTFSE for this answer but nothing came up.shocked
 
 
 
 
    pHarmacist
(Hive Bee)
11-21-02 20:50
No 382119
      yes  Bookmark   

Visit rhodium.ws before asking in forum: ../rhodium /palladium.chloride.txt

"Turn on, Tune in and Drop Out"
 
 
 
 
    jaws
(Newbee)
11-21-02 21:07
No 382127
      jaws  Bookmark   

Jaws just checked this out and it seemes it would be much more simple to just order it. Not that it sounds hard to make but it seems you'd need to many ordered chems. which would defeat the purpose of making it to avoid ordering another chemical.tongue
 
 
 
 
    Organikum
(Hive Bee)
11-21-02 21:10
No 382128
      UTFSE ? if than wrong  Bookmark   

You are not telling the truth or have to inform yourself on the use of the search machine better.
I would say: inform yourself! smile

a tip: search for "lugh" as author of the post.

ORGY

now or never
 
 
 
 
    pickler
(Greenhorn)
11-21-02 21:10
No 382129
      All the chems you need are otc.  Bookmark   

All the chems you need are otc.

I went into the business for the money, and the art grew out of it.-Charlie Chaplin

 
 
 
 
    pupilage
(Newbee)
11-22-02 23:26
No 382524
      palladium chloride  Bookmark   

is costly but not at all a watched chemical. Order from a photo shop and forget about p-benzo do the O2 wacker.
I almost feel like doing a photo work up of how to build a KRV (ketone reaction vessel) just so everyone can see how simple this is. Plus you do not have to remove hydroQ from your ketone so the work up can be done without the Lye wash or if you just have do a NaHO  for nastalgic reasons you can do a 2% wash and not burn up ketone.
The problems that were voiced about O2 wacker early on had to do with failures that came from people trying to do it with out pure O2. They were trying with plain atmosphereic O2 levels at high pressure and there just is not enough O2 to drive the reaction that way so the failures.
Do the Ritter O2 using IPA (it works the best,best yields swim has found so far)
PdCl not watched.
CuCl not watched.
O2 not watched.
O2 from a welding unit is fine almost pure.
O2 wacker is in my book the best way to go for the novice or pro alike.
PdCl is recoverable from the reaction and reusable.
Can you say cost effective.
I know that was off topic but just buy your PdCl and don't worry about it remember you are a home hobbist that wants to develope his own pictures for art sake.

"Sometimes I sits and thinks, and sometimes I just sits." Satchel Paige
 
 
 
 
    GOD
(Hive Addict)
11-22-02 23:35
No 382525
      write-up with pics?  Bookmark   

please do, this synth looks VERY appealing for alot of different reasons, and there is far to little discussion about it here on this board IMO.  Specially since p-Benzo appears to be gaining more and more scrutiny, and oxone is a pain in the ass.

Im not the bearded man upstairs, Im a bald guy with a healthy penis. So open yer pie-hole!
 
 
 
 
    pupilage
(Newbee)
11-23-02 00:40
No 382537
      If Swim does  Bookmark   

Should it be placed in the Methods section or here in NewBee?

"Sometimes I sits and thinks, and sometimes I just sits." Satchel Paige
 
 
 
 
    BlingBling
(Hive Bee)
11-23-02 01:04
No 382539
      an idea..  Bookmark   

Is it possible to use an autoclave for a pressure vessel? I know they are generally rated at 20psi, but that is hot steam, would it be any different if it was pressurized without the heat?

Would the aluminum housing react in any way with the contents?