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pickle11
(Stranger) 11-25-02 19:06 No 383359 |
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magnesium dust in grignard? | Bookmark | |||||
would it be possible to use coarse grade magnesium dust from a fireworks supplier in making grignard reagents. Maybe you would have to wash it first, and add the ether/halobenzene really slowly. |
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Rhodium (Chief Bee) 11-25-02 20:36 No 383373 |
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Yes. Wash with 1 M HCl, then with alcohol, and ... | Bookmark | |||||
Yes. Wash with 1 M HCl, then with alcohol, and finally with ether before using it. |
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