becomezen (Hive Bee)
04-02-03 22:48
No 423396
      post-wacker help needed  Bookmark   

After running the O2 wacker , there is a mixture of PdCl2,CuCl,methanol, and ketone......

Now the problem is , swim has another 9 or so wackers to run (as you can only use 100mL at a time,as per writeup)..

Can swim store this mixture in the freezer , without distilling the tone first ?

Swim wanted to pool together the post-wacker contents and just do 1 distillation rather than 10.....

my guru once told me to "just be" , now I realize he meant "just bee" :)
 
 
 
 
    Antibody2
(Hive Addict)
04-03-03 01:13
No 423429
      absolutely, but a suggestion might be to run a  Bookmark   

absolutely, but a suggestion might be to run a bisulfite test after your 1st wacker to make sure you were in fact sucessful making ketone,  before you go to all that additional effort