pirat (Stranger)
04-18-03 17:58
No 427842
      Is there any downside when i do not distill  Bookmark   

buffered performic
bisulfite addition and recovering à la eleusis without distillation of the ketone!!
al/hg nitro
mdma
this really works

Is there any downside when i do not distill the ketone??
 
 
 
 
    Antibody2
(Hive Addict)
04-18-03 18:37
No 427856
      bisulfite often yeilds gooey crystals that are  Bookmark   

bisulfite  often yeilds gooey crystals that are not really pure, these impurities carry over into subsequent rxns reducing yeild, causing side reactions and complicating further purification. but it can work to some extent

take the search engine out for a test drive there is plenty already posted on the subject