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pooky
(Stranger) 07-05-03 19:28 No 444715 |
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Amalgam or NaBH4 ? | Bookmark | |||||
P just wants to have one success,and then to throw a huge party with free goodies-tested first,naturally.What has the best rate of success for a newbee,amalgam or the borohydride reduction?Sourcing supplies is not a problem,and have double distilled the ketone and have perfect MeNH2 by reading through the Hive and Rhodium's page,with many thanks to LaBTop.Both methods have their good and bad points...anybody with a quick tip?Thanks in advance for your help. |
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raffike (Hive Addict) 07-05-03 20:47 No 444731 |
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certainly borohydride. | Bookmark | |||||
certainly borohydride. For those about to synth,we salute you |
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rudebwoy (Hive Bee) 07-06-03 00:17 No 444767 |
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ehm | Bookmark | |||||
as a newb myself. Trying both rxns. I found that I learned a lot of basics in almagating. Techniques mostly and general understanding of what to do and why to do it. So I think just for the sheer practice of diff techniques I would recommend the amalgation method. Just work it baby! |
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Zero_To_Nine (Stranger) 07-06-03 01:36 No 444782 |
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NaBH4! | Bookmark | |||||
There is nothing easier than a reduction with NaBH4. If you have MDP2P, a good fridge or freezer, IPA and a solution of MeNH2 in alcohol you will get high yields and a relative clean product. The important thing to remember is that the cooler you keep the reaction, the less MDP2Pol will be formed. I have obtained yields up to 90% with this method... |
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terbium (Old P2P Cook) 07-06-03 22:48 No 444972 |
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Borohydride | Bookmark | |||||
If you got it, is far easier and better yielding. All those moments will be lost in time, like tears in rain. |
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