07-25-03 09:31
No 449734
Unbuffered oxone yields the glycol. Buffered oxone yields the expoxide + the glycol which ideally are rearranged seperately. Swim is Pre filtering of course.
For efficiency and yield which method is better, also which rearrangement is better h2so4 or thermal?
I did use tfse, read a bunch and cant seem to draw any definite conclusions, with people on both sides of all of it.
Buffered seems the better of the 2 but barely.
Not a chemist I just follow directions on the box mix
(Hive Addict)
07-27-03 15:04
No 450154
run it buffered. then vac distill your epoxide. Then thermaly rearrange it. it works great.
Start thinking more like a chemist and less like a criminal