alkadelic (Stranger)
02-02-04 07:06
No 485994
      benzo wacker salt washes?     

In step 10. says wash ketone/dcm with sodium bicarbonate in water.(500ml each wash). how much sodium bicarbonate do i add??
In step 11. how much sturated NaCl do i add to(400-500ml) how much water??thanks...
 
 
 
 
    silenziox
(Hive Bee)
02-02-04 07:11
No 485995
      Saturate....     

It's usually good to saturate the solvent with something..
So, dissolve sodium bicarbonate to water until it doesn't
dissolve anymore... Decant or filter to get rid of the solids.

Holotna Pravda... Neskolko dnej iz zhizni siLENZiova   laugh
 
 
 
 
    pooky
(Hive Bee)
02-02-04 20:43
No 486071
      Saturate     

Also use hot water to start,add in way too much and stir the hell out of it.But when making NaOH,use cold water as the reaction is quite exothermic.
 
 
 
 
    Just4Fun
(Stranger)
02-11-04 01:01
No 487761
      A saturated solution is simple.     

A saturated solution is simple. Add as much solid to the solution as it take until no more dissolves.  When no more solid will dissolve remove the excess.