KidCurry (Hive Bee)
05-16-04 12:25
No 507458
       Chlorination of 2,5-DMA?     

Would it be possible to chlorinate 2,5-dimethoxyamphetamine (t o yield DOC) with HCl in tert-butyl hydroperoxide as discussed in the following document: ../rhodium /halosuccinimide.txt ?

I've searched all day, and the alternatives doesn't look that hot, rather avoid liquid chlorine and perchloric acid (NCS-route seemed like a simple procedure otherwise) if I could. :D 		 
 
 
 
    Barium
(Heavyweight Chempion(eer))
05-17-04 00:08
No 507556
       Hmm     

How 'bout UTFSE a bit and look for the alternatives used to make 2C-C (the direct homolog of DOC). I posted something about just that about a year ago. It can't get much easier really.
Severe Aztecoholic and President of Sooty's fanclub - Sooty for President!! 		 
 
 
 
    Rhodium
(Chief Bee)
05-17-04 01:07
No 507564
       Did you ever boost your yields?     

You posted about the Oxone/KCl procedure a while ago: Post 384324 (Barium: "A little 2C-C perhaps", Novel Discourse)

Did you ever boost your yields?
The Hive - Clandestine Chemists Without Borders 		 
 
 
 
    Barium
(Heavyweight Chempion(eer))
05-17-04 01:31
No 507569
       Nah     

I lost interest in that family once I successfully made them. tongue
No oxone halogenation has been performed since that one. If I ever go back to them again I am more interested in making them without having to go through 2C-H or DMA.
I want challenges, damnit!  wink
Severe Aztecoholic and President of Sooty's fanclub - Sooty for President!! 		 
 
 
 
    KidCurry
(Hive Bee)
05-17-04 09:36
No 507651
       Thank you very much! Just one question, in...     

Thank you very much!
Just one question, in you're writeup I suppose you forgot to mention the addition of KCl? Just dissolve KCl and 2,5-DMA in H2O/MeOH and then addition of oxone as in the 2C-I writeup? 		 
 
 
 
    GC_MS
(Hive Addict)
05-17-04 11:28
No 507663
       oxone     

I have never been succesful in chlorination or iodination of 2C-H and 2,5-DMA with oxone and KCl (or KI). On the other hand, I have been succesful in using the same method for bromination of anisole.
WE, THE GOVERNMENT, ONLY PLACED THOSE CAMERAS IN YOUR BEDROOM FOR YOUR OWN PROTECTION 		 
 
 
 
    Barium
(Heavyweight Chempion(eer))
05-17-04 11:59
No 507666
       Nope     

I did not forget to mention the KCl addition. The chloride source was the 2C-H*HCl. It acts as amine source and chloride source at the same time.
Severe Aztecoholic and President of Sooty's fanclub - Sooty for President!!