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pink_dust_angel
(Stranger) 07-28-04 12:49 No 522273 |
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benzyl chloride synth | ||||||
in benzyl chloride synth on rhodiums site how concentrated doesthe HCl have to be? |
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Rhodium (Chief Bee) 07-28-04 14:03 No 522281 |
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Details, please | ||||||
Provide a link and tell us exactly which preparation you are referring to - there are several benzyl chloride syntheses on my page. The Hive - Clandestine Chemists Without Borders |
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pink_dust_angel (Stranger) 07-28-04 17:51 No 522340 |
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i am talking about ../rhodium/chemi... | ||||||
i am talking about ../rhodium /benzylc its the synth that says "Chlorination of benzyl alcohol with conc. HCl " |
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Rhodium (Chief Bee) 07-28-04 17:58 No 522341 |
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10-12 mol/L | ||||||
The stronger acid you use, the higher your yields will be. Concentrated 36-37% HCl is the best to use, but you might get away with using the 31% strength too, just compensate by using a larger excess of acid. The Hive - Clandestine Chemists Without Borders |
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