<a href="https://www.the-hive.ws/forum/showflat.pl?Number=540849&page=0&view=&sort=5&Search=&vc=&new=yes&start=0&xrated=y&&URLForums=" title="Click here to show this downrated post">High boiling fraction</a> (Rated as: UTFSE!) </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post540993"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> pablos (Newbee) 11-11-04 09:59 No 540993 </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> To the "UTFSE " fanatics </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> Maybe I am blind but I can find only information about the terpenes and myristicine,safrole,eugenol,dillapiole fractions but nothing about the rest of the components or bp.in the mace and anethum sowa oils. </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post540998"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> Rhodium (Chief Bee) 11-11-04 10:40 No 540998 </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> The Constituents of the Essential Oil of Nutmeg </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <a href="../methods/000412020.html#Post504015">Post 504015</a> (Rhodium: "The Constituents of the Essential Oil of Nutmeg", Methods Discourse) <hr>The Hive - Clandestine Chemists Without Borders </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post541006"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> pablos (Newbee) 11-11-04 12:30 No 541006 </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> this was really a good read </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> Ok, opssee, I´m a little bit blind. Has nayone reference on anethum sowa too? I got from a really good old eropean source 200 grams of Anethum sowa and 200 grams of Mace claimed with analisis certificate to be respectly 25% dillapiole and 17% myristicine. The amount of dillapiole is "bad", normally range in Europe 40%. The amount of myristicine is really good, normally range in Europe 10%. To good to be true? </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="new_post_bg" title="This is a new post"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post541261"></a><a name="last"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td class="new_post_bg" rowspan="2" title="This is a new post"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> pablos (Newbee) 11-12-04 18:59 No 541261 </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> mace oil distillation </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> Fractional distillation of mace oil report: 100 grams of mace oil claimed to be 17% myristicine was fractional distilled in a 250 ml flask with ~18 torr(calculated with the normograph, with my power 2 fridge pumps vakuum sistem anethole boil at 115~120) Like in the above document posted by Rhodium it can be sayed that the mace oil has 3 great fraction. The first one beginn to distill with approximally 18 toor at 60 C and efinish at approx 100~110 C with a little bit linaol. 74 was collected of a really clear oil. The mixture is passed in a 100 ml flask. The second one fraction beginn with approx. 110~115 C and finish with 155 C.That´s the good one.20 ml was collected, in freezer solidify promptly, have a little yellow tinge. In the flask remain a mass of polimerized crap.Cooled at room temperatur this crap solidify and is really hard to clean.In this moment the flask is seattled in a acetone bad. </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom" class="new_post_bg" title="This is a new post"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> </body> </html>

High boiling fraction , Hive Newbee Forum


		pablos 11-10-04 18:12				<a href="https://www.the-hive.ws/forum/showflat.pl?Number=540849&page=0&view=&sort=5&Search=&vc=&new=yes&start=0&xrated=y&&URLForums=" title="Click here to show this downrated post">High boiling fraction</a> <br> <i title="This post has been downrated by the moderators">(Rated as: UTFSE!)</i> </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post540993"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> pablos<br> <i>(<span title="The user's title at the time of posting">Newbee</span>)</i><br> <span title="Posting date">11-11-04 09:59</span><br> <span title="Link to this post by using the markup [540993]">No 540993</span><br> </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">To the "UTFSE " fanatics</b> </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> Maybe I am blind but I can find only information about the terpenes and <br>myristicine,safrole,eugenol,dillapiole fractions but nothing about the rest of the components or bp.in the mace and anethum sowa oils. </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post540998"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> <font color="#FF0033">Rhodium</font><br> <i>(<span title="The user's title at the time of posting">Chief Bee</span>)</i><br> <span title="Posting date">11-11-04 10:40</span><br> <span title="Link to this post by using the markup [540998]">No 540998</span><br> </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">The Constituents of the Essential Oil of Nutmeg</b> </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> <span title="Jump to this post"><a href="../methods/000412020.html#Post504015">Post 504015</a> <i>(Rhodium: "The Constituents of the Essential Oil of Nutmeg", Methods Discourse)</i></span> <br> <span title="The signature"><hr><sup>The Hive - Clandestine Chemists Without Borders</sup></span> </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post541006"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> pablos<br> <i>(<span title="The user's title at the time of posting">Newbee</span>)</i><br> <span title="Posting date">11-11-04 12:30</span><br> <span title="Link to this post by using the markup [541006]">No 541006</span><br> </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">this was really a good read</b> </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> Ok, opssee,<br>I´m a little bit blind. Has nayone reference on anethum sowa too?<br>I got from a really good old eropean source 200 grams of Anethum sowa and 200 grams of Mace claimed with analisis certificate to be respectly 25% dillapiole and 17% myristicine.<br>The amount of dillapiole is "bad", normally range in Europe 40%.<br>The amount of myristicine is really good, normally range in Europe 10%.<br>To good to be true? </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="new_post_bg" title="This is a new post"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post541261"></a><a name="last"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td class="new_post_bg" rowspan="2" title="This is a new post"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> pablos<br> <i>(<span title="The user's title at the time of posting">Newbee</span>)</i><br> <span title="Posting date">11-12-04 18:59</span><br> <span title="Link to this post by using the markup [541261]">No 541261</span><br> </td> <td rowspan="2"> </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2"> </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">mace oil distillation</b> </td> <td class="text_bg" align="right" valign="top"> </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> Fractional distillation of mace oil report:<br>100 grams of mace oil claimed to be 17% myristicine was fractional distilled in a 250 ml flask with ~18 torr(calculated with the normograph, with my power 2 fridge pumps vakuum sistem anethole boil at 115~120)<br>Like in the above document posted by Rhodium it can be sayed that the mace oil has 3 great fraction.<br>The first one beginn to distill with approximally 18 toor at 60 C and efinish at approx 100~110 C with a little bit linaol. 74 was collected of a really clear oil.<br>The mixture is passed in a 100 ml flask.<br>The second one fraction beginn with approx. 110~115 C and finish with 155 C.That´s the good one.20 ml was collected, in freezer solidify promptly, have a little yellow tinge.<br>In the flask remain a mass of polimerized crap.Cooled at room temperatur this crap solidify and is really hard to clean.In this moment the flask is seattled in a acetone bad. </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom" class="new_post_bg" title="This is a new post"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> </body> </html>