04-04-00 19:53
No 126932
Argh! Right before the end, I posted a list of papers covering Sn2 amine alkylations at DMT World, under my chemistry forum. Wolfsblood seems to have fallen off the planet, and now that the site is pulled, my only copy of these ref's is gone (not to mention half of everything else I had for refrence sources on tryptamines.) Would someone with this list be so kind as to repost it? I'll dig through my hardcopies at home, but it still would be nice to have it already in electronic format.
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-the good reverend drone
Ipsa scientia potestas est
(Junior Member)
04-07-00 15:32
No 126936
(Rated as: excellent)
let's see now, press and ......
Howdy all,
Well, base-promoted Sn2 dialkylation of tryptamines via either alkyl halides or sulfonate esters is certainly a topic in which everybody around here is interested. I've recently come across a fairly large collection of alkylating procedures, and I wanted to share them, so as to further establish the value of this elegant procedure. Enjoy.
Bull.Chem.Soc.Jpn.; 34; 1961; 655-659;
Bull.Soc.Chim.Fr.; 1956; 582, 586;
Chem.Ber.; 43; 1910; 309;
Chem.Ber.; 63; 1930; 804;
Chem.Lett.; 1976; 1149-1152;
Chem.Pharm.Bull.; 8; 1960; 939-944;
Farmaco Ed.Sci.; IT; 17; 1962; 753-772;
Helv.Chim.Acta; 10; 1927; 861;
Helv.Chim.Acta; 20; 1937; 209, 210, 216
Heterocycles; 31; 6; 1990; 1035-1039;
Indian J.Chem.Sect.B; 26; 1-12; 1987; 1121-1123;
J.Amer.Chem.Soc.; 63; 1941; 3135;
J.Amer.Chem.Soc.; 73; 1951; 3325, 3328
J.Amer.Chem.Soc.; 110; 12; 1988; 3862-3869;
J.Biol.Chem.; 164; 1946; 603 Anm. 1;
J.Chem.Soc.; 1960; 4054-4087;
J.Chem.Soc.Chem.Commun.; 17; 1994; 2009-2010;
J.Chem.Soc.Chem.Commun.; 22; 1987; 1690-1691;
J.Med.Chem.; 13; 1970; 254-260;
J.Med.Chem.; 30; 7; 1987; 1144-1149;
J.Org.Chem.; 42; 23; 1977; 3660-3664;
J.Org.Chem.; 56; 13; 1991; 4264-4268;
J.Org.Chem.; 57; 28; 1992; 7175-7187;
J.Prakt.Chem.; 28; 1965; 157-168;
Phosphorus, Sulfur Silicon Relat.Elem.; 109; 1-4; 1996; 237 - 240;
Tetrahedron Lett.; 33; 132; 1992; 1693-1696;
Tetrahedron Lett.; 37; 48; 1996; 8767-8770;
Tetrahedron: Asymmetry; 9; 20; 1998; 3667-3676;
Tetrahedron: Asymmetry; 9; 9; 1998; 1489-1492;
Tetrahedron; 51; 1; 1995; 165-172;
Voila.
Will that do ya, or was there some more after?