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Bandil
(Hive Bee) 10-18-01 02:05 No 226190 |
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Column chromatography of psilocybin! | Bookmark | |||||
Hi! Swim was thinking it would be really cool to have >95% pure psilocybin crystals lying around, as they are quite pretty. Now the mushrooms contain a lot of different alkaloids, that are quire hard(impossible) to separate, by simpel A/B. What about column chromatography: 1) Is silica gel ok for the column? 2) What to use as eluent, DCM, EtOAcOH? 3) I suppose one would have to apply strong vac underneath the column? 4) How to figure out what fractions the psilocybin is in. I was thinking of some TLC(NMR is not an option) Thanks! Regards Peter |
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Rhodium (Chief Bee) 10-18-01 02:07 No 226192 |
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Re: Column chromatography of psilocybin! | Bookmark | |||||
../rhodium /psilo-t |
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lugh (Hive Bee) 10-18-01 08:04 No 226266 |
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Re: Column chromatography of psilocybin! | Bookmark | |||||
And Post 176035 (lugh: "Re: psilocin", Tryptamine Chemistry) ![]() |
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