![]() |
![]() |
|||||||
RDXHMX
(Stranger) 02-10-02 08:26 No 267653 |
![]() |
DMT syntheses 2 | Bookmark | |||||
guys,i`m still working on my little dmt project and looking for some more information en refs. i`m would like to know more about pyrolyses/destillation of the quartenarry ammoniumchloride salt and does any body have any experience with this route,its the first route in pikhal page 412, at the and i will a let you know about my little private project and will wright it all down ,o.k hear from you! ![]() ![]() ![]() |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
RDXHMX (Stranger) 02-10-02 17:02 No 267729 |
![]() |
Re: DMT syntheses 2 | Bookmark | |||||
an other question about this shulgin synthesis the pyrolyses part says to use a "hard" vacuum,howmuch is a "hard" vacuum and can you use a waterjetpump for that or do you need a professional high vacuumpump to reach the needed pyrolyses temperature of 245-250°C,i d`t the first part of the synthesis,tryptamine + iodomethane in 2-propanol and my first rum gave a yield of 92% of that of the shulgin yield,5.45 gram while shulgin got 6.03 gram not bat for a first run. o.k hear from you ![]() ![]() ![]() |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
Lilienthal (Moderator) 02-10-02 19:36 No 267767 |
![]() |
Re: DMT syntheses 2 | Bookmark | |||||
That's a brute force method... Hard vacuum means oil pump vacuum. This will probably yield charcoal if done under water pump pressure. Alternative methods to affect dequaternization are: - boiling with triethanolamine (or was it ethanolamine?) - or LiAlH4 treatment. UTFSE for previous posts on this here in the tryptamine forum. It would be great if somebody could test the (tri)-ethanolamine route on substituted tryptamines ![]() |
||||||||
![]() |
![]() |
|||||||
![]() |
![]() |
|||||||
sunlight (Pioneer Researcher) 02-10-02 19:41 No 267771 |
![]() |
Re: DMT syntheses 2 | Bookmark | |||||
Ethanolamine, a really interesting research but no news till now. Rhodium posted the reference. |
||||||||
![]() |
![]() |
|||||||