03-06-02 03:58
No 277804
To make this shit seems much more easy than to make an amine
out of it.
How many diffrent ways are there for someone that does not have NaBH4?
Yes I have UTFSE and I have found some methods..
1.zink/amalgam
2. palladium on carbon
3. electrolytic reduction
(does anyone know how high the yeld should be fo this?)
Maybee there are some genius here that know more?
(Distinctive Doe)
03-06-02 05:38
No 277820
(Rated as: good read)
Na/Hg
Nitrostyrene reduced to amphetamine
G.A. Alles, Salts of 1-phenyl-2-aminopropane. Patent US1879003 Sept. 1932. C.A. 27: 373 (1933).
LiAlH4
Nitrostyrene reduced to amphetamine
R.T. Gilsdorf and F.F. Nord, Reverse addition of lithium aluminum hydride to nitroolefins.
J. Am. Chem. Soc., 74 (1952) 1837-1843. Post 443723 (GC_MS: "Reverse Addition of LAH to Nitroölefins - A", Novel Discourse)
Raney Nickel (Ni-Al)
Nitrostyrene reduced to amphetamine
J.B. Tindall, Reduction of nitro olefins. Patent US2636901 Apr. 28, 1953. C.A. 48: 2771f (1954).
Nitrostyrene reduced to amphetamine
G. Stochdorph and O. Schickh, Saturated amines. Patent DE848197, Sept. 1, 1952. C.A. 47: 5438b (1953).
Urushibara Ni
../rhodium /amph.ur
Red-Al
../rhodium /red-al.
Al/Hg
../rhodium /znhg.al
diisobutylaluminum hydride (DIBAH)- should work
../rhodium /pheneth
ZnBH4
../rhodium/archive/zinc.boro
Nickel Boride/N2H2
../rhodium /it-290.
Platinum on Carbon
Bacteria
Reduction of nitroolefin using microorganisms.
Chemical and Pharmaceutical Bulletin 38(12), 3449-51 (1990)
Learn to UTFSE and READ RHODIUMS PAGE!
Make a Difference Donate Now!! (http://www.lp.org/drugwar/)
(Chief Bee)
03-06-02 12:25
No 277969
I like the name of the author of the LAH article - F.Nord - very Illuminati-inspired.