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+ADw-title+AD4-Mn Salts For Benzaldehyde Synth
, Hive Chemistry Discourse+ADw-/title+AD4-
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Bwiti
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-Mn Salts For Benzaldehyde Synth+ADw-/b+AD4-
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+ACY-nbsp+ADs- What's up folks?+ACE- Alright, enough of the small talk. U.S. Patent 808,095 uses an Mn salt called mangano-ammonium sulfate in+ACY-nbsp+ADs- H2SO4/H20 to convert+ACY-nbsp+ADs- toluene to benzaldehyde. The Mnammonium sulfate used in the patent is produced by the electrolysis Mnammonium sulfate. I'm not interested in passing a current through a solution to produce this, so what other method can be used? I remember reading somewhere that plain-old manganese(II)sulfate can be converted to the Mn salt and used to convert toluene to benzaldehyde. Assuming that this is true, here's my big question: How can I use KMnO4 to convert the Mnsulfate to Mnsulfate? Or better yet, could Mnacetate be used instead? Btw, could U.S. 808095 be applied to benzene? Peace+ACEAPA-img src+AD0AIg-../forum/images/icons+AF8-lightgrey/cool.gif+ACI- alt+AD0AIg-cool+ACI- title+AD0AIg-Cool+ACI- heigth+AD0AIg-15+ACI- width+AD0AIg-15+ACIAPgA8-br+AD4APA-br+AD4APA-hr+AD4-Love my country, fear my government.
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moo+ADw-br+AD4-
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-Peracetic acid oxidation is mentioned in+ACY-nbsp+ADs-...+ADw-/b+AD4-
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+ACY-nbsp+ADsAPA-a href+AD0AIg-https://www.the-hive.ws/forum/favorites.pl?Cat+AD0AJg-option+AD0-add+ACY-number+AD0-308390+ACY-Number+AD0-308390+ACY-page+AD0-65+ACY-view+AD0AJg-sort+AD0-5+ACY-part+AD0AJg-vc+AD0AJg-new+AD0AJg-backto+AD0-showflat+ACI- title+AD0AIg-Add this post to your bookmark list in your Private Area+ACIAPg-Bookmark+ADw-/a+AD4AJg-nbsp+ADs-
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Peracetic acid oxidation is mentioned in US3992417.
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-Mn(III)acetate +ADw-/b+AD4-
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+ACY-nbsp+ADsAPA-a href+AD0AIg-https://www.the-hive.ws/forum/favorites.pl?Cat+AD0AJg-option+AD0-add+ACY-number+AD0-308514+ACY-Number+AD0-308514+ACY-page+AD0-65+ACY-view+AD0AJg-sort+AD0-5+ACY-part+AD0AJg-vc+AD0AJg-new+AD0AJg-backto+AD0-showflat+ACI- title+AD0AIg-Add this post to your bookmark list in your Private Area+ACIAPg-Bookmark+ADw-/a+AD4AJg-nbsp+ADs-
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There are a lot of posts on Mn(III)acetate both here and on my site, using Mn(II) and KMnO4 as starting materials.
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-Cool, thanks+ACE- I'm thinking I could let a solution ...+ADw-/b+AD4-
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+ACY-nbsp+ADs- Cool, thanks+ACE- I'm thinking I could let a solution of acetic acid, a little H2SO4, and 30+ACU- H2O2 sit for 12 hours, add the Mnammonium sulfate, then wait for the Mn salt to drop out of solution.. Should I replicate what was done in the benzaldehyde patent, by adding the Mn salt to dilute sulfuric before adding the toluene/benzene? Yeah, working with KMnO4/Mn(II)acetate would be easier+ADs- Any reasons why Mn(III)acetate wouldn't produce benzaldehyde? Thanks again+ACE- Peace+ACEAPA-img src+AD0AIg-../forum/images/icons+AF8-lightgrey/cool.gif+ACI- alt+AD0AIg-cool+ACI- title+AD0AIg-Cool+ACI- heigth+AD0AIg-15+ACI- width+AD0AIg-15+ACIAPgA8-br+AD4APA-hr+AD4-Love my country, fear my government.
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