05-27-03 07:20
No 435812
hi :D ... ive searched the lit but i cant find some nmr details for many things... i have many.. but many i dont... does anyone have shift values for mda, mdma? i have suitable reference spectra for the precursers.. but the goodies have been a little difficult to come by...
appreciate your help.
B
(Chief Bee)
05-28-03 03:43
No 435966
Proton and carbon-13 NMR assignments of 3,4-methylenedioxyamphetamine (MDA) and some analogues of MDA
Terry A. Dal Cason, John A. Meyers and David C. Lankin
Forensic Science International 86(1-2), 15-24 (1997) (../rhodium/pdf /mdma-mda.nmr
DOI:10.1016/S0379-0738(97)02102-6
Abstract
Characterization of MDA (3,4-methylenedioxyamphetamine) and a series of nitrogen-substituted MDA analogues has been studied using proton and carbon-13 NMR spectroscopy. The 1H and 13C chemical shift assignments for both have been confirmed using a combination of 1-dimensional and 2-dimensional NMR experiments. The chemical shift trends of the side chain carbon resonances (
-CH2, 
-CH, and 
-CH3) for MDA, N-methyl MDA and N,N-dimethyl MDA, as both free bases and hydrochloride salts, have been examined.Proton and carbon-13 NMR assignments of 3,4-methylenedioxyamphetamine (MDA) and some analogues of MDA
Terry A. Dal Cason, John A. Meyers and David C. Lankin
Forensic Science International 87(2), 175-177 (1997) (../rhodium/pdf/mdma-mda.nmr.
DOI:10.1016/S0379-0738(97)02219-6
Abstract
Errata to Table 1 and 2 in the previous article.
(Newbee)
05-28-03 06:34
No 436004
thankx rhodium, and thanks to however supplied the pdf :D .... much appreciated
(Chief Bee)
05-29-03 00:56
No 436175
Check the link for the second article, I have uploaded that one too now.