lutesium
(Newbee) 08-26-04 20:23 No 527533 |
Sonochemical Barbier Reaction and Oxidation | |||||||
http://nr.stic.gov.tw/ejournal/ChiChemSo Facile Synthesis of Aldehyde and Ketone via Sonochemical Barbier Reaction and Oxidation Lee, Adam Shih-Yuan ; Kung, Chih-Chun Abstract. Methyl ketone is prepared by a sonochemical Barbier reaction of methyl iodide, magnesium powder and aldehyde in Benzene/THF (9/1) solvent in a commercial ultrasonic cleaning bath (39kHz), followed by the addition of N- chlorosuccinimide (NCS) as an oxidizing agent |
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