magstirrer (Stranger)
09-20-04 12:25
No 532358
      Ethyl tosylate data     

Google turns up nothing... anybody has any physical data on this one? Especially boiling/melting point and density...

Thanks in advance :)

[edit] Well, found some minimal info @ alfa-aesar... actually mp only, it is 32-34C ...

BTW CAS number is 80-40-0
 
 
 
 
    KidCurry
(Hive Bee)
09-20-04 12:57
No 532363
      Cut from Chemfinder.com - Density: 1.174 ...     

Cut from Chemfinder.com -
Density: 1.174
Melting point: 34
Boiling point: 158-162 at 10mm Hg

Try searching for ethyl p-toluenesulfonate instead of ethyl tosylate.
 
 
 
 
    roger2003
(Hive Bee)
09-20-04 13:47
No 532369
      Merck 13th     

Title:  Ethyl p-Toluenesulfonate
CAS Registry Number:  80-40-0
CAS Name:  4-Methylbenzenesulfonic acid ethyl ester
Molecular Formula:  C9H12O3S
Molecular Weight:  200.26. 
Percent Composition:  C 53.98%, H 6.04%, O 23.97%, S 16.01%
Line Formula:  CH3C6H4SO3C2H5
Properties:  Monoclinic crystals.  d 1.17.  mp 33°.  bp15 173°.
Melting point:  mp 33°
Boiling point:  bp15 173°
Density:  d 1.17
Use:  For ethylation.

roger2003