acx01b (Newbee)
10-25-04 18:48
No 537715
      very OTC Amph et MethAmph synths     

after reading:
../rhodium /benzylchloride.html
../rhodium /meth.phenylacetaldehyde.html

Toluene is refluxed with dried Ca(ClO)2 to yield BenzylChloride by decantation

Benzylchloride is reacted with Magnesium in very dried diethylether and 2-3mg of iodine to yield BenzylMagnesium Chloride

Acetone is reacted with Ethylamine and microwaved-powdered MgSO4 to yield by phase decantation AcetoneEthylimine

AcetoneEthylimine and BenzylMagnesium Chloride are refluxed to yield after hydrolysis Alpha-Methyl-N-Ethyl-amphetamine (methamphetamine like)
 
 
 
 
    indole_amine
(Hive Bee)
10-25-04 19:11
No 537719
      Ethamphetamine     

Chemistry sounds alright, but N-ethyl-amphetamine is only half as potent as regular amphetamine...


indole_amine
 
 
 
 
    moo
(Hive Addict)
10-25-04 19:35
No 537725
      The product wouldn't be N-ethylamphetamine but     

The product wouldn't be N-ethylamphetamine but N-ethylphentermine.

fear fear hate hate
 
 
 
 
    indole_amine
(Hive Bee)
10-25-04 19:48
No 537730
      reason?     

I guess for n-ethyl-amphetamine one would have to use rather acetaldehyde instead of acetone. Correct?


indole_amine
 
 
 
 
    acx01b
(Newbee)
10-25-04 20:41
No 537746
      it is quite cross-posting but if acetaldehyde...     

it is quite cross-posting but if acetaldehyde is available, this way is cool too:
Ph-CH2-MgCl + CH3CHO --> Ph-CH2-COH-CH3
Ph-CH2-COH-CH3 + H2SO4(90%)/NaCl --> Ph-CH2-CCl-CH3
Ph-CH2-CCl-CH3 can be extracted very easily (phase separation, toluene should work)
then it is reacted with hexamine (pharmacy store)
 
 
 
 
    Bandil
(The Archetypical "Good Guy")
10-25-04 21:37
No 537758
      The reaction of benzylmagnesiumchloride with...     

The reaction of benzylmagnesiumchloride with acetaldehyde will not yield p2pol in any desirable yields. The product will rearrange to something useless (cant remember what), but there are loads of descriptions in TFSE about this...

Only one way leads to Valhalla - Running amok with TOTAL VIKING POWER