Brainpep
(Stranger) 10-25-03 06:29 No 466684 |
Extraktion , Pseudo with Ibuprofen | |||||||
i've got some pills. They have 30mg pseuodo and 200mg Ibuprofen. What would be the best extraktion? Other components: lactosum monohydricum,cellulosum microcristallinium,maydis amylum, carboxymethylamylum natricum, stearinum,silica colloidalis anhydrica,talcum,macrogolum 6000 I've water,dh2o and acetone only. |
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Osmium (Stoni's sexual toy) 10-25-03 08:16 No 466697 |
1) soak crushed pills in first in NP solvent... | |||||||
1) soak crushed pills in first in NP solvent and then acetone; filter, repeat 3 times or more for each solvent 2) dissolve in lots of water, acidify with a little HCl or H2SO4 3) let insolubles settle out at least overnight in a high and narrow container; 24hrs or longer might work even better 4) heat decanted/filtered solution close to boiling point, scoop out shit that might come out of solution 5) extract with non-polar, discard the wash 6) basify with NaOH 7a) extract freebase with NP, evap NP to obtain pseudo freebase In case of horrible emulsion formation: 7b) remove FB by filtration, extract filtercake with hot NP, let evaporate to obtain freebase I'm not fat just horizontally disproportionate. http://www.whatreallyhappened.com |
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