readerror67 (Stranger)
05-24-04 09:41
No 509278
      Wonderland or Nightmare?     

SWIM recently had a dream, and was left with a redish thick liquid in the bottom, uppon adding dh2o, this redish liquid turned into a clear, but yellow tinted liquid, and all the MBRP fell to the bottom. SWIM read the post titled "Re-crystallization via Dual Solvents -Leap Ahead" By Worlock and fallowed the dual solvent instructions, using acetone and isopropyl. In the bottle there is white, fluffy looking things floating around (kind of like liquid myc. for all you mushroom growers). SWIM was wondering if this dream was sucessful or turned into a nightmare, and was also wonder what to do now to get the "substance" out of the liquid if there is any.

Thanks and sorry im stupid.
 
 
 
 
    geezmeister
(Of Counsel)
05-24-04 09:56
No 509279
      errr... ummmm...     

You did extract the meth first and convert it to the salt form, I hope?

mostly harmless
 
 
 
 
    wareami
(Hive Addict)
05-24-04 09:58
No 509280
      Cellulose???     

Does this substance look like a cellulose?
Well no matter!
If the substance of ones desires is dissolved completely in alcohol and these floater are still present, they obviously aren't the objects of desire and need to be removed.
Filter the solution seems like an easy fix.
If it's what Ibee suspects, acetone will make them materialize so be sure adequate tone is available during the filtration process, or the floaters will dissolve again and you'll be back where you started.

a little less conversation, a little more reaction
 
 
 
 
    readerror67
(Stranger)
05-24-04 10:39
No 509292
      Thats what im trying to do, extract the meth.     

Thats what im trying to do, extract the meth.
 
 
 
 
    readerror67
(Stranger)
05-24-04 10:49
No 509296
      I checked the bottle, all of the white shit...     

I checked the bottle, all of the white shit has settled to the bottom, Any idea wtf it could be? I think I messed up, I put the iso/tone into the post reaction+dh20, Is it saveable?
 
 
 
 
    readerror67
(Stranger)
05-24-04 10:59
No 509298
      Sorry to keep replying, but I thought this...     

Sorry to keep replying, but I thought this might be important, The 'white shit' didnt appear until after it was heated and it became more when it reached a slight boil...

People like me deserve to be shot due to stupidity....
 
 
 
 
    geezmeister
(Of Counsel)
05-24-04 11:21
No 509302
      That's what I feared...     

I think you got ahead of yourself. You tried to recrystallize before you extracted the meth from the post reaction fluid.

I suggest you read this: Post 428410 (geezmeister: "The post-reaction workup: a cook's summary", Stimulants) It should answer a lot of your questions.

mostly harmless
 
 
 
 
    readerror67
(Stranger)
05-24-04 12:31
No 509314
      Yea, I probably did, but I went to the store,...     

Yea, I probably did, but I went to the store, grabbed some lye and added ice, dh20, lye, yellow shit and VM&P Naptha, shook, the top layer turned blue(wtf?), I think the top layer is the water and the bottom is the naptha? Which one should I use?
 
 
 
 
    kris_1108
(Hive Bee)
05-24-04 13:12
No 509317
      You need to read some more     

It appears to me that you don't quite know what you're doing.

After the reaction, the meth has to bee extracted from the yellow reaction fluid with an ACID/BASE EXTRACTION. AND THEN YOU CAN RECRYSTALIZE IT!

Have a really good read of that link that Geezmeister posted for you.
 
 
 
 
    ici_rhi
(Hive Bee)
05-24-04 16:13
No 509364
      Re: think the top layer is the water and the...     


I think the top layer is the water and the bottom is the naptha? Which one should I use?




Wrong guess. If you want to "use" the naptha by titrating it, use the layer on top. The one that smells like naptha.

(You did use hot naptha, didn't you?)

Wash it the way suggested in the writeup Geezmeister pointed you to, then titrate it as he describes.

But don't throw anything away just yet.


mystic slut of lore