psilly1
07-12-04 23:43 |
(Rated as: UTFSE!) |
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NaXen (Stranger) 07-13-04 01:18 No 518997 |
.... | |||||||
add a little bit more water and reflux it. 250C sounds pretty excessive, try to stay ~100. you may have fried your mix and will probably need to start over, refluxing is the easiest way to go with a small rxn like that IMHO |
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psilly1 (Stranger) 07-13-04 01:30 No 518999 |
Do you think adding more I2 would help if no... | |||||||
Do you think adding more I2 would help if no traces can be seen in the flask?? FUK GAKK!!! |
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NaXen (Stranger) 07-13-04 02:04 No 519004 |
it it was all sublimed, then you would need... | |||||||
it it was all sublimed, then you would need fresh stuff. BUT the E is probably toasted...you could try putting new I2, add a little water and just cook/reflux it at about 100C for however long you want- longer is better. you may or may not get anything, depending on how much E survived. the only thing thats probably still alright is the RP. check out some of the links in the 'Stimulants FAQ' for more info |
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