11-07-01 07:52
No 234167
Has anyone come up with a good suggestion on what to use for the DMF O2 Reaction Vessel? I have searched around and everyone seams to have Ghetto rigged with no clear winner on what to use. I have been researching talking to Glassblowers even yet no one really seams to Know. Plastic it seams will wear out. SS is a no go but for a 4L reaction Vessel nobody seams to know proper thickness and stuff. Anyone have an answer?
(Hallucinogenius)
11-07-01 11:15
No 234201
Glass filter carboys are made of some of the thickest borosilicate you will find and they have held 3 atmospheres on a consistent basis. Plenty of reaction volume as well. Or just get a glasteel pfaulder 10 gallon RX-series w/ helical impeller... mmmmmmmmmmmm chem porn... ahhhhhh........
(Newbee)
11-07-01 14:22
No 234275
carboys good idea didn't think of that one thanks. 3 atmospheres is how many psi? thanks
what are you goofy?
(Newbee)
11-07-01 17:43
No 234353
thanks madmax a regular round bottom flask can't take that pressure. swim knows from experience.
what are you goofy?
(Hive Bee)
11-07-01 20:02
No 234424
if you want to scale up use a ss paint sprayer with overhead stirring, and included psi gauge. oh yeah use a hdpe bucket inside for reagents or you're fucked!
hope this helps
j
"fuck the media"
(Hive Bee)
11-09-01 01:03
No 234860
Don't use the bucket inside. When it gets hot, the steam goes over the edge and you lose water.
Use this, teflon coated:
Free Strike too.
(Hive Elder)
11-09-01 09:37
No 234897
The wacker will NOT work with very pleasing results if done in a stainless vessle, expect enough "tar" and shit to re-pave your driveway. As Grouch mentioned telfon coat that puppy and you should be fine...
Mean People Suck