chinone (Stranger)
09-24-02 09:10
No 359859
      Sodium Triacetoxyborohydride Reductive Amination  Bookmark   

Has anyone tried this? If so what were the results and conditions used?
 
 
 
 
    Organikum
(Hive Bee)
09-24-02 11:14
No 359882
      yes. daily between 8:30 and 9:00 am. why ask?  Bookmark   


http://www.callery.com/pdf/bulletin/calselect_stab.pdf

under "applications" is listed what this compound maybe used for.

ORGY

~ Love is the law, love under will. ~
 
 
 
 
    Rhodium
(Chief Bee)
09-24-02 17:13
No 359981
      ../rhodium/pdf/sodium.  Bookmark   

../rhodium/pdf /sodium.triacetoxyborohydride.pdf
 
 
 
 
    slappy
(Hive Bee)
10-02-02 19:20
No 363282
      Triacetoxy has been used, and was found to give ...  Bookmark   

Triacetoxy has been used, and was found to give very favorable results.

1 eq. NaBH(OAc)3 in 47.5/47.5/5 Dichloroethane(DCE)/THF/AcOH and amine freebase.