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topdowner
10-17-03 18:56
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<a href="https://www.the-hive.ws/forum/showflat.pl?Number=465222&page=14&view=&sb=&Search=&vc=&new=&start=0&xrated=y&&URLForums=" title="Click here to show this downrated post">satisfy a solution with HCl gas</a>
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<i title="This post has been downrated by the moderators">(Rated as: UTFSE!)</i>
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<td colspan="7"><a name="Post465773"></a></a> </td>
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sYnThOmAtIc<br>
<i>(<span title="The user's title at the time of posting">Hive Addict</span>)</i><br>
<span title="Posting date">10-20-03 18:21</span><br>
<span title="Link to this post by using the markup [465773]">No 465773</span><br>
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<b title="The subject of this post">You mean saturate? ../rhodium/chemis...</b>
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You mean saturate? And how did you ever manage to make 2,5DMA without knowing how to liberate gasses from acid solutions?<br><br><a href="../rhodium
/hcl-gas.html" target="_blank" title="Jump to this external site">../rhodium
/hcl-gas<wbr>.html</a>
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<span title="The signature"><hr>Yes, That pic really is me!</span>
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politoxicomania<br>
<i>(<span title="The user's title at the time of posting">Newbee</span>)</i><br>
<span title="Posting date">10-29-03 18:16</span><br>
<span title="Link to this post by using the markup [467574]">No 467574</span><br>
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<b title="The subject of this post">MeOH / HCl Solution</b>
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English:<br>Put Ammoiumchloride in a 250 ml roundbottom 2-neck flask and fit a funnel at one neck. Fill this Funnel with konc. Sulfuric Acid and let drop it slowly to the Ammoniumchlorid. Gaseuos HCl will form and u can let this go through the other neck into a flask with MeOH. <br><br>Better in German:<br>Man nehme einen 250ml 2hals rundkolben und lege Ammoniumchlorid vor. Über einen Tropftrichter ohne Druckausgleich lässt man langsam konz. Schwefelsäure zutropfen. Das entstehende HCl lässt man über den zweiten Hals in einen zweiten Kolben durch MeOH leiten.(Waschflasche eignen sich sehr gut dafür). Man schaltet eine zweite Waschflasche hinter die erste und beschickt diese mit einem Wasser/Indikator Gemisch, um zu Überwachen dass kein HCl in die umgebung entweicht und wann das Methanol gesättigt ist ......<br><br>Good Luck
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