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+ADw-title+AD4-wanna make trans-4-mar with me+ACE- I just started it
, Hive Methods Discourse+ADw-/title+AD4-
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trans4mar
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OK i just started to reflux my PPA/KOCN mix.+ADw-br+AD4APA-br+AD4-Using a +ADw-br+AD4-Gram condenser(i think, its the bubble one)+ADw-br+AD4APA-br+AD4-Hot Plate from wal-mart with small frying pan with olive oil in it.+ADw-br+AD4APA-br+AD4-500ml FB Flask+ADw-br+AD4APA-br+AD4-Cheap water pump from home depot and a 3 gallon bucket for the water/ice being pumped through the condenser. Using 2 frozen bottles of water to chill the water.+ADw-br+AD4APA-br+AD4-28Grams of phenylpropanolamine(C9H13NO)HCI was added to 150mls or so of hot water in the flask.+ACY-nbsp+ADs- Still looks like water+ACEAJg-nbsp+ADs- +ADw-br+AD4APA-br+AD4-Then put in 12 grams potassium cyanate +ACU-97 and mixed well. Still looks like water+ACEAPA-br+AD4APA-br+AD4-Just put it on to reflux.+ACY-nbsp+ADs- I used this PVC tape to seal the condenser with the flask. HD has it in the plumbing section. Its black and seals it water tight. Love this stuff.+ADw-br+AD4APA-br+AD4-The reflux is going at 130deg C. cause the condenser cant handle the 140deg reflux. should be no problem.+ACY-nbsp+ADs- Its refluxing nicely. +ADw-br+AD4APA-br+AD4-Plus some kids are playing in front of my garage/lab and i dont have to worry about blowing them up. LMAO+ADw-br+AD4APA-br+AD4-Hold for update on step two...........
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trans4mar+ADw-br+AD4-
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Ok.....+ADw-br+AD4APA-br+AD4-I have the 32+ACU-hcl from home depot. I used just about 1cup(200ml) disolved into 1ltr of water for my 2m solution????????? anyway+ADw-br+AD4APA-br+AD4-Into the flask i poured about 200ml water and then about 200ml of the 2m solution. I should have used less water cause i didnt wait too cool down and filter. O well we will see what happens
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trans4mar+ADw-br+AD4-
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well i let the last reflux run about 3hours at around 130deg.+ACY-nbsp+ADs- I let it cool down overnight.+ACY-nbsp+ADs- Still just looks like water+ACEAPA-br+AD4APA-br+AD4-Now I have always felt like i was fckin up the last step cause my flask always turns milk white once i add my 20+ACU- sodium carbonate solution.+ACY-nbsp+ADs- Trying to filter through coffee filters sucks too+ACEAPA-br+AD4APA-br+AD4-SO THIS TIME i just let the milky flask sit for the day. When i came back all the powder was on the bottom so i poured most of the water off then poured the rest on a plate to dry.+ACY-nbsp+ADs- +ADw-br+AD4APA-br+AD4-11grams dry yeild.+ADw-br+AD4APA-br+AD4-THen i took some thinner(from HD) with toulene in it and heated to a nice boil.+ACY-nbsp+ADs- I pour the powder in and let boil for a second till everything had disolved.+ACY-nbsp+ADs- If everything doesnt disolve let it settle cause that shit is just junk on the bottom. Then i poured off the liquid onto a plate and left the solids in the flask.+ADw-br+AD4APA-br+AD4-After evaporation the crystals are almost clear and you can see them sparkle from across the room+ACEAJg-nbsp+ADs- Looks 10x better than the pure ISO recryst.+ADw-br+AD4APA-br+AD4-Sorry about the grammer and sentence structure. Im one spun monkey right now and i cant spell for shit+ACEAPA-br+AD4APA-br+AD4-I still rather have some good old meth though+ACE-
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