12-24-02 19:34
No 392620
does anyone know if it is best to mix the 02 wacker chems first then add the saferole or is it best to put them together all at the same time?
(Greenhorn)
12-24-02 20:29
No 392634
You need to premix the pdcl2 in the meoh first. It takes a little bit of time to disolve. Then add your cupric. Then safrole.
I went into the business for the money, and the art grew out of it.-Charlie Chaplin
(Hive Bee)
12-25-02 17:16
No 392848
which 02 method are you guys referring to?
Theres nothing to be afraid of, just concentrate, and trust the music.
(Hive Bee)
12-25-02 17:23
No 392851
uh, the one that used o2, pdcl2 and cucl...
(Stoni's sexual toy)
12-31-02 14:29
No 394573
Dissolve the PdCl2 AND CuCl2 together in the MeOH. It's faster that way.
I'm not fat just horizontally disproportionate.
(Hive Bee)
12-31-02 15:03
No 394583
PdCl2 in MeOH for at least 8 hours before adding CuCl2 into the PdCl2 mixture. Then add the Olefin of choice.
"Sometimes I sits and thinks, and sometimes I just sits." Satchel Paige
(Stoni's sexual toy)
12-31-02 16:12
No 394597
Nope.
I'm not fat just horizontally disproportionate.