k0dog
(Stranger) 05-19-03 00:55 No 434035 |
Can someone please explain something to me? =) | Bookmark | ||||||
I haven't been on in a long time but was reading over one of my old posts... and realized I have no clue the exact conditions (temp.) for converting: 1-hydroxycyclophenyl-(2-Cl-Ph)-ketone-N- Also if swim had a HCl salt of that compound (1-hydroxycyclophenyl-(2-Cl-Ph)-ketone-N "Vanity is defintely my favourite sin" -Devil's advocate |
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k0dog (Stranger) 05-19-03 00:59 No 434036 |
Sorry... did some searching and found | Bookmark | ||||||
I doid some searching... (afterwards sorry) and found that it takes 180 C for 30 min.... sorry... But for the 2nd part of the question... whats the answer.... "Vanity is defintely my favourite sin" -Devil's advocate |
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Rhodium (Chief Bee) 05-19-03 01:44 No 434047 |
Salt or freebase? | Bookmark | ||||||
You would very likely have to freebase it before performing the thermal rearrangement, as the imine which you now have in its salt form is at the very center of where the rearrangement of the molecule is going to take place. |
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