05-28-03 16:40
No 436087
Don't ask how it happened, I wasn't there so I really don't know. But here is the problem.
Basically, after drying with Mag. Sulfate, about 100mls of methanol was accidently added (always label your shit). So, now swim has a solution containing DCM, ketone, and methanol.
The question is should he go ahead and wash it again, or can he just distil? Tried to look it up with TFSE, but nothing specific to this question.
GT
"The gods are too fond of a joke." (Aristotle)
(Hive Addict)
05-28-03 19:30
No 436112
just distill and it'll be fine,no harm done
For those about to synth,we salute you
(Newbee)
05-29-03 20:04
No 436370
Correct me if I'm wrong, but couldn't you just wash with water as well? save yourself distillation time. everything seems to be nonpolar except the alcohol
(Hive Addict)
05-31-03 00:15
No 436656
That's what he was thinking, but he hated losing anymore product than he has to. He lost a lot due to a fuckin emulsion.
Interesting, very interesting.....
Regular distilled was with maybe 300mls. What do you think?
"The gods are too fond of a joke." (Aristotle)