Aphexx (Stranger)
10-15-03 04:25
No 464777
      A/B Mescaline Extraction - Xylene Alternative?  Bookmark   

SWIM has been using xylene to perform a successful defatting of cactus material, however is now finding difficulty in obtaining more xylene for the basification step. I have read procedures that involve DCM and methanol, but is there a common solvent with the same properties as xylene that would be effective as a replacement for the basification step that SWIM still needs to perform? Thanks smile
 
 
 
 
    Bandil
(you can always take some more)
10-15-03 04:31
No 464779
      I think that DCM is more efficient for ...  Bookmark   

I think that DCM is more efficient for defatting process, as it is a somewhat more agressive than xylene for instance. As solvent for the A/B extraction toluene or ethylacetate is probably two good alternatives. DCM will give you a less pure extraction, as it pull's almost everything non-polar over in the organic phase, but it works smile. Methanol is not useable here, as it is miscible with both water and almost whatever you throw at it(except the pure carbon solvents like heptane, hexane etc).

I just love the smell of bromine in the morning!