Swim is doing a MM benzo wacker(1/2 ... , Hive Newbee Forum
 
    edo 02-13-04 18:36
       <a href="https://www.the-hive.ws/forum/showflat.pl?Number=488511&page=29&view=&sort=5&Search=&vc=&new=&start=0&xrated=y&&URLForums=" title="Click here to show this downrated post">Swim is doing a MM benzo wacker(1/2 ...</a> <br> <i title="This post has been downrated by the moderators">(Rated as: UTFSE!)</i> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post488814"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> pickler<br> <i>(<span title="The user's title at the time of posting"><font color=green>Greenhorn</font></span>)</i><br> <span title="Posting date">02-15-04 03:07</span><br> <span title="Link to this post by using the markup [488814]">No 488814</span><br> </td> <td rowspan="2">  </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">Yup, your on the right track.</b> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> Yup, your on the right track. <br> <span title="The signature"><hr>I went into the business for the money, and the art grew out of it.-Charlie Chaplin <br><br></span> </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post488816"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="1"> </td> <td rowspan="1"> </td> <td valign="top" align="center" rowspan="1"> edo<br> <span title="Posting date">02-15-04 03:23</span><br> </td> <td rowspan="1">  </td> <td rowspan="1" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="1">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post"> <a href="https://www.the-hive.ws/forum/showflat.pl?Number=488816&page=29&view=&sort=5&Search=&vc=&new=&start=0&xrated=y&&URLForums=" title="Click here to show this downrated post">thx pickler, I did use TFSE</a> </b><br> <i title="This post has been downrated by the moderators">(Rated as: insignificant)</i> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post488824"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> edo<br> <i>(<span title="The user's title at the time of posting">Stranger</span>)</i><br> <span title="Posting date">02-15-04 04:35</span><br> <span title="Link to this post by using the markup [488824]">No 488824</span><br> </td> <td rowspan="2">  </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">Shit! Swim doing mm wacker and forgot to dry...</b> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> Shit! Swim doing mm wacker and forgot to dry his ketone with 50g magnesium sulfate and he already distilled. Is that a big deal? </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post488850"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="1"> </td> <td rowspan="1"> </td> <td valign="top" align="center" rowspan="1"> wyndowlicker<br> <span title="Posting date">02-15-04 08:03</span><br> </td> <td rowspan="1">  </td> <td rowspan="1" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="1">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post"> <a href="https://www.the-hive.ws/forum/showflat.pl?Number=488850&page=29&view=&sort=5&Search=&vc=&new=&start=0&xrated=y&&URLForums=" title="Click here to show this downrated post">HEy now,</a> </b><br> <i title="This post has been downrated by the moderators">(Rated as: insignificant)</i> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post488862"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> <font color="#FF0033">Rhodium</font><br> <i>(<span title="The user's title at the time of posting">Chief Bee</span>)</i><br> <span title="Posting date">02-15-04 09:43</span><br> <span title="Link to this post by using the markup [488862]">No 488862</span><br> </td> <td rowspan="2">  </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">Distilling without drying</b> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> Distilling without drying <b>works</b>, but may cause troublesome bumping in the process, and the water will be sucked into your pump, reducing its efficiency. <br> <span title="The signature"><hr><sup>The Hive - Clandestine Chemists Without Borders</sup></span> </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post489882"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> edo<br> <i>(<span title="The user's title at the time of posting">Stranger</span>)</i><br> <span title="Posting date">02-19-04 20:07</span><br> <span title="Link to this post by using the markup [489882]">No 489882</span><br> </td> <td rowspan="2">  </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">shit, Swim should of washed with H2O a few...</b> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> shit,<br> Swim should of washed with H2O a few times after the NaOH wash. the whole thing turned in a big black chard<img src="../forum/images/icons_lightgrey/frown.gif" alt="frown" title="Frown" heigth="15" width="15">(polymerized) Swim smashed the flask to save magnetic stirr bar.   <br>Swim still learning the hard way </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post489889"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> amine<br> <i>(<span title="The user's title at the time of posting">Hive Bee</span>)</i><br> <span title="Posting date">02-19-04 20:42</span><br> <span title="Link to this post by using the markup [489889]">No 489889</span><br> </td> <td rowspan="2">  </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">did you try removing the gunky mess with ...</b> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> did you try removing the gunky mess with hotwater before attempting to smash the flask? generally hot/boiling water will get the tar out.<br>;) </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post489904"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> Bond_DoubleBond<br> <i>(<span title="The user's title at the time of posting">Newbee</span>)</i><br> <span title="Posting date">02-19-04 22:45</span><br> <span title="Link to this post by using the markup [489904]">No 489904</span><br> </td> <td rowspan="2">  </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">refluxing some dcm in the flask works ...</b> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> refluxing some dcm in the flask works extremely well to remove that tar.  or if you wanna be lazy, put some dcm in the flask and run some hot water over the flask until the dcm starts boiling and swirl it around a bit.  and if you don't wanna use your solvent dcm, you can get dcm containing (>80%) paint and adhesive removers from just about any hardware store for pretty cheap.<br><br>once your washing techniques start to improve, you won't get much of that tarry shit.  swim considers h2o washes to be essential after washing with any acid or alkaline solution.  and don't just stop with one water wash.  perform h2o washes until the ph of the aqueous phase is near neutral. </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> <td align="left" valign="top" class="text_bg"> <img src="../forum/images/left_top.gif" border="0" height="12" width="9"></td> <td colspan="7"><a name="Post490062"></a><a name="last"></a></a> </td> <td align="right" valign="top"><img src="../forum/images/right_top.gif" border="0" height="12" width="9"></td> </tr> <tr class="text_bg"> <td rowspan="2"> </td> <td rowspan="2"> </td> <td valign="top" align="center" rowspan="2"> edo<br> <i>(<span title="The user's title at the time of posting">Stranger</span>)</i><br> <span title="Posting date">02-20-04 15:35</span><br> <span title="Link to this post by using the markup [490062]">No 490062</span><br> </td> <td rowspan="2">  </td> <td rowspan="2" width="1" class="vert_ruler"> <img src="../forum/images/hr.gif" border="0" width="1" height="1"> </td> <td rowspan="2">  </td> <td class="text_bg" align="left" valign="top"> <b title="The subject of this post">Swim knew to was with H2O after NaOH wash but...</b> </td> <td class="text_bg" align="right" valign="top">    </td> <td> </td> </tr> <tr class="text_bg"> <td colspan="2" valign="top" align="left"> <br> Swim knew to was with H2O after NaOH wash but swim was tired as shit and forgot. Swim will remember the hot water/DCM to remove tar.(Hopefully never again)<br>Swim shouldn't have rushed but Swim had success first time making ketone and was eager to repeat it.<br>thx </td> <td> </td> </tr> <tr class="text_bg"> <td align="left" valign="bottom"><img src="../forum/images/left_bottom.gif" border="0" height="12" width="9"></td> <td valign="middle" align="center" colspan="7"> </td> <td align="right" valign="bottom"><img src="../forum/images/right_bottom.gif" border="0" height="12" width="9"></td> </tr> <tr class="page_bg"> <td colspan="9"> </td> </tr> </body> </html>