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+ADw-title+AD4-Salting mescaline with dilute sulphuric acid?
, Hive Newbee Forum+ADw-/title+AD4-
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KidCurry
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-Salting mescaline with dilute sulphuric acid?+ADw-/b+AD4-
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Purely theoretically, if one could not obtain concentrated sulphuric acid and would need to make a salt of mescaline, would it be possible to use cold battery acid (35-38+ACU- H2SO4) since mescaline sulfate has a low solubility in cold water (cool the acid before in freezer for a few minutes, and add it to a beaker on an icebath)?
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It should work. I use 50:50 water/conc sulfuric acid (v/v) to crystallize mescaline freebase as the sulfate. Calculate how much solution you need though. Better not loose too much of the precious M +ADw-img src+AD0AIg-../forum/images/icons+AF8-lightgrey/wink.gif+ACI- alt+AD0AIg-wink+ACI- title+AD0AIg-Wink+ACI- heigth+AD0AIg-15+ACI- width+AD0AIg-15+ACIAPg-.
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+ADw-span title+AD0AIg-The signature+ACI-+AD4APA-hr+AD4--+- THE GOVERNMENT IS YOUR FRIEND -+-+ADw-/span+AD4-
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If battery acid is all you can get I would just make the citrate form out of a solution of citric acid, battery acid can be pretty dirty it could contain lead and shouldn't be consumed with a hallucinogen, a strong one at that. Or you could make a dilute solution of HCL to make mescaline hcl+ADw-br+AD4APA-br+AD4-either which way the salt should be washed and recrystallized to improve purity
+ADw-br+AD4-
+ADw-span title+AD0AIg-The signature+ACIAPgA8-hr+AD4-Isolation is a must for the experimentation of a model subject.+ADw-/span+AD4-
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-I thought new battery acid was just dilute...+ADw-/b+AD4-
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I thought new battery acid was just dilute sulphuric acid without additives? I don't mean acid taken out from a battery, but the acid you buy to refill them. +ADw-br+AD4-And what's the solubility of M-HCl in water? I thought it was a lot mor soluble than the sulfate salt.+ADw-br+AD4APA-br+AD4-Recrystallisation/washing would of course be done.
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Refill battery acid will probably work, it might or might not have a some additives depending where it came from, but it should be suitable for the task. What color is it? can you see any insolubles in the acid floating around?
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+ADw-span title+AD0AIg-The signature+ACIAPgA8-hr+AD4-Isolation is a must for the experimentation of a model subject.+ADw-/span+AD4-
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-I haven't actually got any yet.+ADw-/b+AD4-
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I haven't actually got any yet. This is purely theoretical thoughts. But if someday the synthesis of mescaline will become legal where I live, and I aquire some battery acid I will check for impurites and what the label says.+ADw-br+AD4APA-br+AD4-Thanks for the help everybody, really appreciate it+ACE- :)
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Smilaxium+ADw-br+AD4-
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+ADw-b title+AD0AIg-The subject of this post+ACIAPg-Add methanol ?+ADw-/b+AD4-
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I was just wondering if adding methanol to a 50/50 mixture of H2SO4 and H2O would reduce the amount of amphetamine that is dissolved...And even that would not be my first choice. Still you will loose too much precious crystals+ACE-
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+ADw-span title+AD0AIg-The signature+ACIAPgA8-hr+AD4-The light at the end of the tunnel is usually a +ACY-quot+ADs-No Exit+ACY-quot+ADs- sign.+ADw-/span+AD4-
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