beeach
(Member) 04-29-00 10:27 No 108889 |
Delepine Dreaming | Bookmark | ||||||
Well, I was wondering if anyone had any success with the Delepine for MDA. Here is what Egotrip posted about making DMMDA and I wanted to try for MDA. Can anyone post some specific amounts and a way to do it room temperature without the reflux? General procedure is safrole -> bromosafrole -> iodosafrole -> Delepine (hexamine) -> MDA 1) 25 g dillapiole The dmso was frozen,solid. Removed from icebox. Chilled H2SO4 was added to the dmso With vigorous stirring, the dillapiole is dripped into the dmso/sulfuric/nabr mixture, which, The rate is a slow one, taking about an hour to get it all in, keeping it cool in a bath. yield was about 70% 90%!! Both of these reactions are very general and can be successfully performed. Methylamine But heres what swim did; put the undistilled iodo-cmpd in 10x amount of alcohol by wt. Refluxing this for 6 hours gave an eventual yield of DMMDA-2 which is quite rewarding. No one should doubt the power of delepine! Add HCl until the ph is 2. The red liquid is evaporated until a mass of hard rocklike crystals remained. This is impure DMMDA-2. The crystals CANNOT be cleaned, with ether or any other Freebase and distill to give clear, off colored dmmda-2. The yield is 50 % from the beginning. SWIM got ~12 g at the end. Happy Trails! |
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