Vibrating_Lights
(Hive Addict) 06-19-03 04:28 No 441002 |
Synthesis of PMDEA | Bookmark | ||||||
11ml diethylamine is dissolved in 30ml MeOh with 2 gms silica gel in an ice bath. then 10gms of PMP2P is alled and stirred for 1 hr. then .83 gms NaBH4 is added all at once and stirred for 20 hrs. 5ML GAA is added and solution is washed with 20mlDCM. Product basified with 10 ml25% Naoh An extracted with 30 ml EtAcOh 2x. theses extracts are dried and gassed with HCl to give 8gms P-Methoxyphenyl-2-diethylamine. Mp.Pending rextyl. I wonder what this is going to do?? VL_ Start thinking more like a chemist and less like a criminal |
||||||||
Rhodium (Chief Bee) 06-19-03 06:34 No 441009 |
A cautionary note | Bookmark | ||||||
Whatever it may do, be careful with the dosage - as you know, many mono-oxygenated amphetamines have significant pressor activity (i.e. increases heart rate and blood pressure) compared to their psychoactive effect - so a toxic dose may be lower than the dose needed to produce a significant psychoactive effect. Other than this cautionary note, nice to see someone developing novel substances. |
||||||||
Vibrating_Lights (Hive Addict) 06-19-03 14:13 No 441125 |
Bioassay | Bookmark | ||||||
Bioassay will come when optical isomers are isolated and analyzed with GC/MS. Will start bioassay at 250mcg. DEA stinks. easy synth though liquid amines are cool. Many twisted analogs to come since the DEA is requiring permits now. Start thinking more like a chemist and less like a criminal |
||||||||