Solvent | Formula | 1H shifts | 13C shifts | mp °C | bp °C |
Acetic Acid | CD3COOD | 2.2 | 21.1, 177.3 | 16.6 | 117.9 |
Acetone | CD3COCD3 | 2.09 | 30.7, 205.1 | -94.7 | 56.1 |
Acetonitrile | CD3CN | 2.0 | 0.3, 117.2 | -43.8 | 81.6 |
Benzene | C6D6 | 7.4 | 128.7 | 5.5 | 80.1 |
Carbon Disulphide | CS2 | none | 192.8 | -11.6 | 46.3 |
Carbon Tetrachloride | CCl4 | none | 96.7 | -23.0 | 76.8 |
Chloroform | CDCl3 | 7.3 | 77.05 | -63.5 | 61.3 |
Dichloromethane | CD2Cl2 | 5.3 | 54.2 | -95.1 | 40.8 |
Diethyl Ether (-100 °C) | (CH3CH2)2O | ?, 66.51 | -116.3 | 34.6 | |
Dimethyl Ether (-100 °C) | CH3OCH3 | 3.2 | 60.08 | -138.5 | -23 |
Dimethylformamide | Me2NCHO | 31, 36, 162.4 | -61.? | 153.? | |
Dimethylsulfoxide | CD3SOCD3 | 2.6 | 39.6 | 18.6 | 189.0 |
1,4-Dioxan | (OCH2CH2)2 | 3.7 | 67.8 | 11.8 | 101.4 |
Ethanol | CD3CD2OD | 1.2, 7.3, 3.8 | 17.9, 57.3 | - | 78.3 |
Methanol | CD3OD | 3.5 | 49.3 | -97.8 | 64.6 |
Nitrobenzene | C6D5NO2 | 7.5, 7.7, 8.1 | 123, 129, 135 | 5.7 | 210.8 |
Nitromethane | CD3NO2 | 4.3 | 57.3 | -28.6 | 101.2 |
Pyridine | C5D5N | 7.1, 7.6, 8.8 | 123.9, 135.9, 150.2 | -41.6 | 115.3 |
1,1,2,2-Tetrachloroethane | CHCl2CHCl2 | ? | 75.5 | -43.8 | 146.3 |
Tetrahydrofuran | C4H8O | 1.8, 3.7 | 26.7, 68.6 | -108.5 | 65.4 |
Tetrahydrofuran -100 °C | ?, 67.96 | ||||
Toluene | C6D5CD3 | 2.1, 7.0-7.1 | 20.4, 124-137 | -94.9 | 110.6 |
Trichlorofluoromethane | CFCl3 | none | 117.6 | -111 | 23.7 |
Trifluoroacetic Acid | CF3COOD | ~10 | 99-136,162-167 | -15.3 | 72.4 |
Water | D2O | 4.8 | none | 0.0 | 100.0 |
Solvent | Formula | 1H shifts | 13C shifts | mp °C | bp °C |